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As a result, the Ti decreases drastically in the process of heating as the nitrogen oxide and vapor are quickly unveiled accompanying the thermal decomposition of nitrogen-containing compounds at minimal temperatures [21], which can be confirmed via the TG-IR benefits. Furthermore, it truly is truly worth noting that FR-PA66 demonstrates two decomposition peaks when compared with pure PA66, as well as Tmax2 is higher than the Tmax1 of pure PA66 no matter the information of HCNP. This phenomenon may very well be due to the dehydration response of CNHO teams along with the dehydrogenation reaction of α-CH2 facilitated through the R-P· no cost radical substances developed from HCNP, accelerating the development from the protective compact char levels [22].
On the other hand, the steady multilayer carbonaceous chars (Figure 5) created from the response in between HCNP and the decomposition products and solutions of PA66 can insulate the fundamental substrate from your warmth source and decelerate each the heat and mass transfer [25]. Hence, it can be summarized that HCNP can effectively Increase the flame retardancy of PA66 following the gasoline-phase flame retardant system.
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Concerning the TGA success of FR-PA66, the Tmax1 little by little shifted to the lower temperature than that from the neat PA66 with rising HCNP mainly because of the very low Ti of pure HCNP. Figure 1c displays the Ti of HCNP is 352 °C due to the P-N bond precedence breakage concerning HCCP and DABA underneath decreased temperatures. It is actually fascinating to view which the P-made up of alkanes of FR-PA66 are detected via the TG-IR exam less than 400 °C, which can be considerably unique through the thermal decomposition items of pure PA66 [20]. Also, the R-P· radicals produced by HCNP can catalyze and speed up the breaking of C-N bonds at the α place from the PA66 molecular chain, causing the development of unstable amino radicals and carbonyl radicals, leading to the decomposition of your FR-PA66.